Nano pores evolution in hydroxyapatite microsphere during spark plasma sintering

Simulation of thermal and electric field evolution during spark plasma sintering

Finite element simulations have been conducted to determine the temperature distribution (both in radial and axial direction), heat and electric flux-field in the powder compact/die/punch assembly during the spark plasma sintering (SPS) process. A thermal–electrical coupled model with temperature dependent thermal and electrical properties is implemented. The simulation studies were conducted u...

Chemical analysis of silica doped hydroxyapatite biomaterials consolidated by a spark plasma sintering method.

Silica (SiO(2)) and the silicate-based biomaterials play an important role due to their in vitro and in vivo biological response. The present study synthesized a novel nano-structured amorphous silica doped hydroxyapatite (HA) via an aqueous precipitation route. HA was prepared with 0, 1, 3 and 5 wt% silica, which are comparable to the measured silicon content of natural bone. After spray dryin...

Characterization of Multiwalled Carbon Nanotube-Reinforced Hydroxyapatite Composites Consolidated by Spark Plasma Sintering

Pure HA and 1, 3, 5, and 10 vol% multiwalled carbon nanotube- (MWNT-) reinforced hydroxyapatite (HA) were consolidated using a spark plasma sintering (SPS) technique. The relative density of pure HA increased with increasing sintering temperature, but that of the MWNT/HA composite reached almost full density at 900°C, and then decreased with further increases in sintering temperature. The relat...

Effect of Nano-TiN on Mechanical Behavior of Si3N4 Based Nanocomposites by Spark Plasma Sintering (SPS)

Spark Plasma Sintering of Negative Temperature Coefficient Thermistor Ceramics